反応 #9487

反応方程式

7-Bromo-4-chloro-3-nitroquinoline

3-methoxy propyl amine

→

(7-bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine

収率 94.2%

反応条件

実験手順

7-Bromo-4-chloro-3-nitroquinoline (29.54 g, 102.7 mmol) was reacted with 3-methoxy propyl amine (10.07 g, 113.0 mmol) according to the method described in Part A of Examples 125–135 to provide 32.9 g of (7-bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine as a yellow solid. The product was not recrystallized.

出典