反応 #944003

ord-b0a4a8e63efb465f9411668e6efe4ed1

反応方程式

CSc1ccc(N=Cc2ccc(C)cc2)cc1
N-(4-methylbenzylidene)-4-methylthioaniline
C[Si](C)(C)C#N
trimethylsilyl cyanide
CSc1ccc(NC(C#N)c2ccc(C)cc2)cc1
title compound
CSc1ccc(NC(C#N)c2ccc(C)cc2)cc1
α-(4-Methylphenyl)-α-(4-methylthioanilino) acetonitrile

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Following a procedure similar to that described in Example 1(ii), but using N-(4-methylbenzylidene)-4-methylthioaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a pale yellow powder (yield 73%).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: USRE039420E1uspto-grants-2006_12