反応 #94362

反応方程式

Ammonia

benzophenone

benzoic acid

→

benzophenoneimine

収率 26.0%

溶媒

o-dichlorobenzene

反応条件

後処理

1. 1
   その他was passed through the reaction mixture under 6 atmospheres at 160° C. of the reaction temperature at a feed rate of 0.2 l/min. (NTP)

実験手順

36.2 Grams of benzophenone, 50 ml of o-dichlorobenzene and 0.5 g of benzoic acid were fed to a reactor. Ammonia gas was passed through the reaction mixture under 6 atmospheres at 160° C. of the reaction temperature at a feed rate of 0.2 l/min. (NTP) continuously. The reaction was conducted for 3 hours and benzophenoneimine was obtained in yield of 26%.

出典