反応 #94361

反応方程式

benzophenone

benzoic acid

ammonia

→

benzophenoneimine

収率 65.0%

反応条件

後処理

1. 1
   workup.ADDITIONdispersing plate at a feed rate of 2 l/min. at a reaction temperature of 200° C
2. 2
   その他Reaction

実験手順

91.1 Grams of benzophenone and 0.1 g of benzoic acid were charged into a pressure reactor, and an ammonia gas under 8 atmospheres was continuously fed to the reactor through a gas dispersing plate at a feed rate of 2 l/min. at a reaction temperature of 200° C. Reaction was carried out for 2 hours. As a result, benzophenoneimine was obtained in yield of 65%.

出典