反応 #94102

反応方程式

dimethyl adipate

sodium hydroxide

→

disodium adipate

溶媒

acetonitrile

反応条件

後処理

1. 1
   温度at reflux temperature for 18 hours
2. 2
   ろ過The resulting solution was filtered hot
3. 3
   その他dried

実験手順

17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.

出典