反応 #939017

反応方程式

mono-perphthalic acid

mono-perphthalic acid

sodium sulfite

→

2-Butylsulfonylcyclopentanone

溶媒

ether

反応条件

後処理

1. 1
   洗浄the resultant solution was washed
2. 2
   その他evaporated
3. 3
   その他to remove the solvent
4. 4
   workup.DISTILLATIONdistilled

実験手順

2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).

出典