反応 #93804

反応方程式

6-chloro-nicotinic acid

SOCl2

→

6-chloronicotinoyl chloride

反応条件

実験手順

Starting from 250 g 6-chloro-nicotinic acid and 850 ml SOCl2, and using the working conditions as in Ex. 1a, there is obtained 243 g 6-chloronicotinoyl chloride, m.p. 49°-51° C.; b.p. 75° C./0,05 mm.

出典