反応 #93595

反応方程式

methyl angelate

(Z)-3-hexenyl alcohol

dioctyltin laurate

→

(Z)-3-Hexenyl Angelate

溶媒

toluene

反応条件

後処理

1. 1
   workup.ADDITIONA mixture of 20.0 g
2. 2
   その他glass flask, which was equipped with a Soxhlet extractor

実験手順

A mixture of 20.0 g. of methyl angelate, 26.34 g. of (Z)-3-hexenyl alcohol, 100 ml. of toluene and 1.2 g. of dioctyltin laurate was placed in a 300 ml. glass flask, which was equipped with a Soxhlet extractor filled on the top with molecular sieve 4A and a reflux cooler.

出典