反応 #93594

反応方程式

methyl angelate

3-methyl-3-butenyl alcohol

dioctyltin laurate

→

3-methyl-3-butenyl Angelate

溶媒

toluene

反応条件

後処理

1. 1
   workup.ADDITIONA mixture of 20.0 g
2. 2
   workup.DISTILLATIONThe reaction mixture was subjected to single distillation
3. 3
   その他to obtain 39.5 g

実験手順

A mixture of 20.0 g. of methyl angelate, 22.65 g. of 3-methyl-3-butenyl alcohol, 100 ml. of toluene and 0.8 g. of dioctyltin laurate was reacted under the same conditions as in Example 6. The reaction mixture was subjected to single distillation to obtain 39.5 g. of a distillate boiling at 104° C. (32 mmHg).

出典