反応 #93481

ord-bde75dd99363429981065e3c265be9d8

反応方程式

Clc1ncc(-c2ccccc2Cl)nn1
3-chloro-6-(2-chlorophenyl)-1,2,4-triazine
Cl.O.O=C1CCNCC1
piperidin-4-one monohydrate hydrochloride
O=C([O-])[O-].[Na+].[Na+]
sodium carbonate
O=C1CCN(c2ncc(-c3ccccc3Cl)nn2)CC1
6-(2-Chlorophenyl)-3-(4-oxopiperidino)-1,2,4-triazine

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

1.5 g of 3-chloro-6-(2-chlorophenyl)-1,2,4-triazine, 3.05 g of piperidin-4-one monohydrate hydrochloride and 3.1 g of sodium carbonate are heated under reflux in 100 ml of ethanol for 4 hours.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04613603uspto-grants-1986_09