反応 #934669

反応方程式

butane-1,4-diol

trimethylchlorosilane

→

1,4-bis-trimethylsiloxybutane

反応条件

後処理

1. 1
   workup.DISTILLATIONThe product was worked up by fractional distillation

実験手順

1 mole of butane-1,4-diol, 3 moles of trimethylchlorosilane and 0.002 moles of tributyl-hexadecyl phosphonium bromide were reacted at the reflux temperature (56°-96° C.) as in Example 1. The product was worked up by fractional distillation.

出典