反応 #9346

反応方程式

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

溶媒

Triflic Acid

反応条件

後処理

1. 1
   その他The resulting waxy solid was purified by chromatography on silica gel

実験手順

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

出典