反応 #93319
ord-1d11c5876e414d0185f4cd42bc97df70
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度The suspension was refluxed for 8 hours
- 2その他Excess volume of thionyl chloride was evaporated off under reduced pressure
実験手順
In 6 ml of thionyl chloride was suspended 5.0 g of piperonylic acid. The suspension was refluxed for 8 hours. Excess volume of thionyl chloride was evaporated off under reduced pressure to give crude crystals of piperonylic acid chloride.