反応 #926693

反応方程式

3,4-dihydro-6,7-dimethoxyisoquinoline hydrochloride

3,4-dihydroisoquinoline hydrochloride

1-cyclopenten-1-yl methyl ketone

→

2,3,4,4a,6,7,11b,12,13,13a-decahydro-9,10-dimethoxy-1H-dibenzo[a,f]quinolizin-13-one

溶媒

methyl ketone

反応条件

実験手順

When in Example 32 appropriate amounts of 3,4-dihydro-6,7-dimethoxyisoquinoline hydrochloride and 1-chylohexen-1-yl methyl ketone respectively are substituted for 3,4-dihydroisoquinoline hydrochloride and 1-cyclopenten-1-yl methyl ketone, 2,3,4,4a,6,7,11b,12,13,13a-decahydro-9,10-dimethoxy-1H-dibenzo[a,f]quinolizin-13-one is obtained M.P. 129°-141° C.

出典