反応 #92497

反応方程式

Compound 7p

3-(4-(3,4-dichlorophenyl)piperazine-1-yl)propan-1-ol

triphenylphosphine resin

imidazole

iodine

→

1-(3,4-dichlorophenyl)-4-(3-iodopropyl)piperazine

溶媒

DCM

反応条件

後処理

1. 1
   その他The product compound 11p was used without further purification for the next reaction

実験手順

Compound 7p was mixed with triphenylphosphine resin, imidazole and iodine in DCM as described in General Procedure B. The product compound 11p was used without further purification for the next reaction. MS (LC/MS, ESI): 399 (M+H).

出典