反応 #91963

反応方程式

3-methyl-4-[(2-methylpropan-2-yl)oxycarbonyl]morpholine-3-carboxylic acid

trifluoroacetic acid

→

3-methylmorpholine-3-carboxylic acid

溶媒

DCM

反応条件

後処理

1. 1
   濃縮concentrated under the vacuum
2. 2
   その他The residue was used directly in next step without further purification

実験手順

To a solution of 3-methyl-4-[(2-methylpropan-2-yl)oxycarbonyl]morpholine-3-carboxylic acid (Accela ChemBio Co., Ltd., CAS: 1052680-53-1, 50 mg, 0.2.0 mmol) in DCM (1 ml) was added trifluoroacetic acid (1 mL) dropwise at room temperature. The resulting mixture was stirred at room temperature for one hour and then concentrated under the vacuum. The residue was used directly in next step without further purification,

出典