反応 #90932

反応方程式

5H-[1,3]dioxolo[4,5-f]indole-6-carboxylic acid

4-(benzyloxy)-2-methylbenzaldehyde

benzo[d][1,3]dioxole-5-carbaldehyde

→

6-(Benzyloxy)-4-methyl-1H-indole-2-carboxylic acid

反応条件

後処理

1. 1
   その他Intermediate I-5a was prepared

実験手順

Intermediate I-5a was prepared using procedures analogous to those described above for the synthesis of 5H-[1,3]dioxolo[4,5-f]indole-6-carboxylic acid (I-4c) using 4-(benzyloxy)-2-methylbenzaldehyde (I-4c) as the starting material instead of benzo[d][1,3]dioxole-5-carbaldehyde. ESI MS: m/z 282.24 (M+H).

出典