反応 #90078

ord-dc0aec06b9fc4d80a246b2df75c94f8d

反応方程式

COc1ccc2c(c1)CCC(=O)C2
6-methoxy-3,4-dihydro-1H-naphthalen-2-one
CI
iodomethane
COc1ccc2c(c1)C(C)(C)C(=O)CC2
Compound A2
COc1ccc2c(c1)C(C)(C)C(=O)CC2
7-Methoxy-1,1-dimethyl-3,4-dihydro-1H-naphthalen-2-one
→
COc1ccc2c(c1)CCC(=O)C2(C)C
title compound
COc1ccc2c(c1)CCC(=O)C2(C)C
6-Methoxy-1,1-dimethyl-3,4-dihydro-1H-naphthalen-2-one

反応物

COc1ccc2c(c1)CCC(=O)C2
6-methoxy-3,4-dihydro-1H-naphthalen-2-one
CI
iodomethane
COc1ccc2c(c1)C(C)(C)C(=O)CC2
Compound A2
COc1ccc2c(c1)C(C)(C)C(=O)CC2
7-Methoxy-1,1-dimethyl-3,4-dihydro-1H-naphthalen-2-one

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Under the same conditions as the method for synthesizing Compound A2, the title compound was prepared from 6-methoxy-3,4-dihydro-1H-naphthalen-2-one and iodomethane.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US09440922B2uspto-grants-2016_09