反応 #8986

ord-4a51539e54e6499c8098a02ac20b71d4

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The title compound was prepared in accordance with the literature reference of Cliff & Pyne, Synthesis-Stuttgart (7), 681–682(1994) by reacting 2-cyclopropyl-1H-imidazole with iodine in the presence of NaOH. The obtained 4,5-diiodo-2-cyclopropyl-1H-imidazole was then reacted with sodium sulfite to obtain the title compound.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07091222B2uspto-grants-2006_08