反応 #89797

ord-0e9e4199149b43188a2b7b866cc8e30c

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Step A is conducted starting from 2,2′-diethylhexylamine and α-chlorophenylacetyl chloride and leads to 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide (Yield: 96%) for which the characterisations by 1H and 13C NMR are given below:

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US09441285B2uspto-grants-2016_09