反応 #88243

反応方程式

benzylamine

4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide

→

title compound

4-(benzylamino)benzo[d][1,2,3]triazine-8-carboxamide

反応条件

後処理

1. 1
   その他Compound 6 was prepared

実験手順

Compound 6 was prepared following general synthetic scheme 7 wherein benzylamine was reacted with 4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide to give the title compound. LC-MS [280 (M+1)], 1H NMR (400 MHz, DMSO-d): δ 9.42 (s, 1H), 9.31 (t, 1H), 8.53 (t, 1H), 8.04 (s, 1H), 7.98 (t, 1H), 7.41 (d, 2H), 7.34 (t, 2H), 7.28-7.24 (m, 1H), 4.92 (d, 2H).

出典