反応 #86631

反応方程式

6-(3-(triethoxysilyl)propylthio)hexyl 2-bromo-2-methylpropanate

sodium iodide

→

6-(3-(triethoxysilyl)propylthio)hexyl 2-iodo-2-methylpropanate

溶媒

acetone

反応条件

後処理

1. 1
   その他to react in a nitrogen atmosphere at 75° C. for 10 hours
2. 2
   その他After the reaction, extraction

実験手順

The 6-(3-(triethoxysilyl)propylthio)hexyl 2-bromo-2-methylpropanate (5 g) obtained through the procedures of Example 1 was mixed with sodium iodide (20 g) and dry acetone (100 mL), and the mixture was allowed to react in a nitrogen atmosphere at 75° C. for 10 hours. After the reaction, extraction was performed to give 6-(3-(triethoxysilyl)propylthio)hexyl 2-iodo-2-methylpropanate of the chemical formula below (compound 6).

出典