反応 #84840

反応方程式

2-(4-bromo-3,5-dimethoxyphenyl)furan

2-ethoxy-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide

→

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-ethoxy-2-(4-morpholinophenyl)ethanone

反応条件

後処理

1. 1
   その他Purification by chromatography (50% EtOAc/hexanes)

実験手順

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-ethoxy-2-(4-morpholinophenyl)ethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and 2-ethoxy-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (50% EtOAc/hexanes) gave the product as a yellow solid (0.129 g, 34% yield). MS: m/z 530.2 [M+H]+.

出典