反応 #8407

ord-b2a7a735024242189307b0a478130651

反応方程式

CNC(=O)c1c(C)noc1-c1ccccc1
3-methyl-5-phenyl-isoxazole-4-carboxylic acid methylamide
COC(=O)c1ccc(C=O)cc1
4-formyl-benzoic acid methyl ester
COC(=O)c1ccc(-c2cc3noc(-c4ccccc4)c3c(=O)n2C)cc1
4-(5-Methyl-4-oxo-3-phenyl-4,5-dihydro-isoxazolo[4,3-c]pyridin-6-yl)-benzoic acid methyl ester

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他This compound is obtained

実験手順

This compound is obtained using 3-methyl-5-phenyl-isoxazole-4-carboxylic acid methylamide and 4-formyl-benzoic acid methyl ester in 15% as a beige solid. Mass spectrum: m/z (M+H)+: 361.2

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07087756B2uspto-grants-2006_08