反応 #84025

反応方程式

Oxalyl chloride

t-butyl alcohol

→

Compound 34

Chloro-Oxo-Acetic Acid t-Butyl Ester

溶媒

ether

反応条件

後処理

1. 1
   その他The solvent was evaporated under vacuum

実験手順

Oxalyl chloride (232 μL, 2.8 mmol) and t-butyl alcohol (228 μL) were combined in ether (6.7 mL) under nitrogen at 0° C. The resulting mixture was stirred for 30 minutes at room temperature. The solvent was evaporated under vacuum to form Compound 34.

出典