反応 #83757

反応方程式

methyl 7-azaindol-1-acetate

lithium aluminum hydride

→

title compound

収率 87.1%

2-(7-Azaindol-1-yl)ethanol

収率 87.1%

溶媒

tetrahydrofuran

反応条件

後処理

1. 1
   その他A procedure similar to that described in Preparation 2

実験手順

A procedure similar to that described in Preparation 2 was repeated, except that 7.50 g of methyl 7-azaindol-1-acetate (prepared as described in Preparation 17), 1.80 g of lithium aluminum hydride and 260 ml of anhydrous tetrahydrofuran were used, to give 5.57 g of the title compound, melting at 52.7°-53.3° C.

出典