反応 #833510

反応方程式

Vanillin

allyl bromide

potassium carbonate

→

3-methoxy-4-(2-propenyloxy)benzaldehyde

溶媒

acetone

反応条件

後処理

1. 1
   温度After cooling
2. 2
   ろ過the solid was filtered off
3. 3
   洗浄washed with acetone
4. 4
   その他A yellow oil was obtained
5. 5
   濃縮after a thorough concentration of the organic phases

実験手順

Vanillin (20.0 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.

出典