反応 #83341

反応方程式

2-(4-Aminophenylthio)-6-chloroquinoline

4-chloro-3-trifluoromethylphenylisothiocyanate

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title compound

収率 51.3%

1-[4-(6-Chloro-2-quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

収率 51.3%

反応条件

実験手順

2-(4-Aminophenylthio)-6-chloroquinoline (2.9 mmoles, 0.83 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (3.2 mmoles, 0.76 g) were reacted according to procedure C to yield 0.78 g, 51% of the title compound. Mass Spec (FD) 524. Calculated for C23H14ClF3N3S2 : C, 52.68; H, 2.69; N, 8.01. Found: C, 52.66; H, 2.78; N, 7.91. M Pt 138°-139° C.

出典