反応 #8315

反応方程式

3-benzyl-4-bromo-butyric acid

thionyl chloride

→

3-benzyl-4-bromo-butyryl chloride

収率 127.0%

反応条件

後処理

1. 1
   その他The thionyl chloride is evaporated

実験手順

A mixture of 3-benzyl-4-bromo-butyric acid (2.0 g, 7.78 mmol) and thionyl chloride (6.0 mmol) is heated to 80° C. for 2 h. The thionyl chloride is evaporated to yield 3-benzyl-4-bromo-butyryl chloride 2.1 g (99%), as a colorless liquid.

出典