反応 #828717

ord-124348c9e3c74a01bcdfa140f15247e0

試薬

なし

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他After the completion of the reaction
  2. 2
    その他After separating the lower layer from the upper layer
  3. 3
    その他to obtain D-HPAE, which

実験手順

After the completion of the reaction, an extractant such as ethyl acetate is added to the reaction mixture which separates the reaction mixture into an upper layer and a lower layer. The upper layer contains D-HPAE in the organic solvent and the lower layer contains L-HPA in water. After separating the lower layer from the upper layer, the extractant, i.e., ethyl acetate, can be vaporized to obtain D-HPAE, which can be chemically hydrolyzed to obtain D-homophenylalanine.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05552317uspto-grants-1996_09