反応 #828710
ord-63b60552a7b74907b643503b04151a11
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
236faE (CAS Reg. No. 20193-67-3) has been prepared by reaction of 2,2,2-trifluoroethanol with carbonyl fluoride to give the intermediate, CF3CH2OCOF, which was in turn reacted with sulfur tetrafluoride at 150°-200° C. to give the product as disclosed by Eisemann in U.S. Pat. No. 3,394,878.