反応 #82703
ord-7f7b3066bbb14fee89758dd2e71988a4
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度to warm slowly overnight
実験手順
A THF solution (10 mL) of 3,6-dichloropyridazine (16.8 mmol, 2.5 g) was added dropwise to a solution of lithium tetramethylpiperidine (20.1 mmol) in 170 mL of THF at -78° C. After one hour at -78° C., tributyltin chloride (21.8 mmol, 5.8 mL) was added to the anion solution and the solution was allowed to warm slowly overnight.