反応 #82144

ord-165c21acb8a34d9c9681683a969f54e5

反応物

試薬

なし

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    ろ過The polymer was filtered
  2. 2
    抽出The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor
  3. 3
    その他dried
  4. 4
    その他to afford a pale brown solid which

実験手順

The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05621088uspto-grants-1997_04