反応 #818363

反応方程式

47.2

5-Bromo-2,3-dihydro-1H-inden-1-ol

thionyl chloride

→

5-Bromo-1-chloro-2,3-dihydro-1H-indene

溶媒

DCM

反応条件

後処理

1. 1
   その他After evaporation of solvent
2. 2
   その他47.3 was obtained
3. 3
   その他it was used without further purification

実験手順

A mixture of 47.2 (11.1 mmol) and thionyl chloride (44 mmol) in DCM (20 mL) was stirred at room temperature overnight. After evaporation of solvent, 47.3 was obtained and it was used without further purification.

出典