反応 #816373

反応方程式

4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one

N-(3-hydroxyphenyl)acetamide

ammonia

→

N-{(6E)-6-[(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)imino]-3-oxocyclohexa-1,4-dien-1-yl}acetamide

溶媒

water

2-propanol

反応条件

後処理

1. 1
   その他ranging from 5 to 10° C.

実験手順

10 mmol of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in 30 ml of water. This solution was admixed with 10 mmol of N-(3-hydroxyphenyl)acetamide in solution in 30 ml of 2-propanol, 3 ml of 20% aqueous ammonia and 22 mmol of potassium ferricyanide at a temperature ranging from 5 to 10° C.

出典