反応 #81578

ord-2cfee49587a7491f9b68ddf95299674a

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Starting with benzenesulfonyl chloride and the mixture of regioisomers of 5-chloro-2-(2-hydroxyethyl)-7-[(2,4,6-trimethylphenyl)methoxy]anthra-[1,9-cd]pyrazol-6(2H)-one II and 5-chloro-2-(2-hydroxyethyl)-10-[(2,4,6-trimethylphenyl) methoxy]anthra-[1,9-cd]pyrazol-6(2H)-one III, using the procedure of example 3, the title compound was prepared.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05618944uspto-grants-1997_04