反応 #806269

反応方程式

triethylammonium 2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate

HCl

→

2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate

溶媒

water

water

反応条件

後処理

1. 1
   workup.ADDITIONwas added
2. 2
   ろ過the resultant mixture was filtered
3. 3
   洗浄The residue was washed with water (20 mL)

実験手順

A triethylammonium 2-(6-cyano-1-hexyn-1-yl)adenosine 5′-monophosphate (1.1 g) was dissolved in water (20 mL), and, under ice-cooling conditions, 1N HCl solution (2 mL) was added thereto, followed by standing for 10 minutes. After having been diluted with water (20 mL), the resultant mixture was filtered. The residue was washed with water (20 mL) and then with ethanol (20 mL×2), to thereby yield 617 mg of the above-titled compound as a colorless amorphous substance.

出典