反応 #806245

ord-c7694efff96c41abbebbcd9625f0d7f2

反応方程式

Oc1ccccc1
phenol
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)O
sulfuric acid
Oc1ccccc1
Phenol
Oc1ccccc1
phenol
Oc1ccccc1
phenol
Oc1ccccc1
Phenol
O=S(=O)(O)c1ccc(O)cc1
phenolsulfonic acid

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

A treatment for canker sores was formulated. A solution of phenolsulfonic acid was prepared as described in Example 1, except that the weight of available stock liquefied phenol USP was calculated and prepared for 2.4 moles of phenol. The amount of available stock sulfuric acid NF that contained 5.26 moles was calculated. The weight of sulfuric acid NF was 515.90 grams. The 5.26 moles of sulfuric acid NF was treated as described in Example 1. A quantity of 400 mL of Liquified Phenol USP was added to a 600 mL beaker. A quantity of 2.4 moles of phenol as Liquefied Phenol USP was added to a 1 L Corning Pyrex No. 1395 bottle using the Mettler PS-5002-S balance.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07132111B2uspto-grants-2006_11