反応 #806242

反応方程式

guaiacol

sulfuric acid

sulfuric acid

sulfuric acid

guaiacol

guaiacol

guaiacol

→

guaiacolsulfonic acid

溶媒

water

Water

反応条件

後処理

1. 1
   その他The weight of available stock guaiacol, purified reagent, that
2. 2
   その他purified reagent from the available stock bottle
3. 3
   workup.ADDITIONwas added to the bottle

実験手順

A solution of guaiacolsulfonic acid in sulfuric acid was prepared. Water in the recirculating water bath was heated to 65 degrees Centigrade. The weight of available stock guaiacol, purified reagent, that contained 1.63 moles of guaiacol was calculated. The amount of available stock of sulfuric acid NF that contained 3.41 moles of sulfuric acid was calculated. A 1 liter Corning Pyrix bottle No. 1395 was placed on the Mettler PG-5002-S balance. A 600 mL beaker was filled with approximately 400 mL guaiacol, purified reagent from the available stock bottle. A quantity of 1.63 moles of guaiacol as guaiacol, purified reagent by weight from the beaker was added to the bottle.

出典