反応 #80365

ord-e07dd7275ae142a087005e26d2ce40e0

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Following a procedure similar to that described in Example 34, but using N-[4-(4-piperidinomethyl-2-pyridyloxy) -cis-2-butenyl]-4-chlorobutyramide (prepared as described in Preparation 2) and 2-mercaptopyridine as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as an oil in a 53% yield.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05616579uspto-grants-1997_04