反応 #77734

反応方程式

Carbazole

boron trifluoride etherate

→

9-acetyl-carbazole

溶媒

acetic anhydride

反応条件

後処理

1. 1
   温度the solution refluxed for 25 min.
2. 2
   その他the solid was then collected
3. 3
   その他recrystallized from hexane

実験手順

Carbazole (100.24 g) was suspended in acetic anhydride (300 mL) with catalytic boron trifluoride etherate (0.65 mL) and the solution refluxed for 25 min. then cooled to 0° C. and the solid was then collected and recrystallized from hexane to give 82.65 g 9-acetyl-carbazole.

出典