反応 #7657

ord-e8614edd65754b1d8eb7b12fffa62985

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The crude product is used in the next step without further purification

実験手順

In analogy to the procedure for Example 36A, 150 mg (0.67 mmol) 6-(1-aminopropyl)-3-cyclopentyl-1,2,4-triazin-5(4H)-one, 90 mg (0.74 mmol) 2,2-dimethylpropanoyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07087605B2uspto-grants-2006_08