反応 #7638

反応方程式

6-(1-aminopropyl)-3-cyclopropyl-1,2,4-triazin-5(4H)-one

cyclopentanecarbonyl chloride

→

N-[1-(3-Cyclopropyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclopentanecarboxamide

反応条件

後処理

1. 1
   その他The crude product is used in the next step without further purification

実験手順

In analogy to the procedure for Example 36A, 250 mg (1.29 mmol) 6-(1-aminopropyl)-3-cyclopropyl-1,2,4-triazin-5(4H)-one, 170 mg (1.29 mmol) cyclopentanecarbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.

出典