反応 #76222

反応方程式

1-chlorobutane

1-methylimidazole

→

1-butyl-3-methylimidazolium chloride

収率 98.3%

反応条件

後処理

1. 1
   workup.WAITThe mixture is left
2. 2
   その他to react for 24 h at 80° C
3. 3
   その他The reaction mixture is evaporated under vacuum

実験手順

251.4 g of 1-chlorobutane (2.7 mol) are loaded into a 1 l glass reactor. The mixture is heated to 60° C., and then 148.6 g of 1-methylimidazole (1.8 mol) are poured in dropwise, with stirring. The mixture is left to react for 24 h at 80° C. The reaction mixture is evaporated under vacuum. 309 g of 1-butyl-3-methylimidazolium chloride are obtained in the form of a yellowish solid (yield=98%). The product is used as it is without further purification.

出典