反応 #75648
ord-d3e2222c3045443591698a2b7c600b99
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Compound 15 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol styrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile. Subsequent saponification was carried out using 1.0 ml of sodium hydroxide solution (6N water) in 20.0 ml of ethanol.