反応 #75647

反応方程式

3,5-dichloroaniline

ethylglyoxalate

styrene

trifluoroacetic acid

→

Compound 14

5,7-dichloro-4-phenyl-1,2,3,4-tetrahydroquinoline-2-carboxylic Acid Ethyl Ester

溶媒

acetonitrile

反応条件

実験手順

Compound 14 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol styrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.

出典