反応 #75645

反応方程式

3,5-dichloroaniline

ethylglyoxalate

2-vinylnaphthalene

trifluoroacetic acid

→

Compound 11

収率 84.0%

5,7-dichloro-4-naphthalene-2-yl-1,2,3,4-tetrahydroquinoline-2-carboxylic Acid Ethyl Ester

収率 84.0%

溶媒

acetonitrile

反応条件

実験手順

Compound 11 was prepared in a yield of 84% by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol 2-vinylnaphthalene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.

出典