反応 #7552

反応方程式

carbonate

oxalic acid

→

carbonate oxalate

溶媒

ethyl acetate

ethyl acetate

反応条件

後処理

1. 1
   その他The crystals precipitated
2. 2
   ろ過were collected by filtration

実験手順

In 7 mL of ethyl acetate was dissolved 0.31 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate, and to the solution was added a solution of 0.10 g of oxalic acid in 1 mL of ethyl acetate, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.34 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate oxalate.

出典