反応 #75022

ord-3c2d463041064f17a5965d17a1397be7

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    温度heated under nitrogen in 300 ml

実験手順

Octene-1 in an amount of 3.37 g. and 4.8 g. of freshly prepared MnO2.4H2O were mixed with and heated under nitrogen in 300 ml. glacial acetic acid containing 90 g. potassium acetate. After a reaction time of less than two hours, gamma-n-hexyl-butyrolactone was obtained in 74% yield.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04175089uspto-grants-1979_11