反応 #74890
ord-1a06f9ffbc2c46afaf47b657be09d7f6
反応方程式
5-Nitroacenaphthene
nitric acid
tin
hydrazine
acenaphthene
→
5-aminoacenaphthene
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
5-Nitroacenaphthene is made by nitrating acenaphthene with nitric acid in the presence of acetic acid according to the method of Rowe and Davies, J. Chem. Soc. 117, 1346 (1920). Standard reduction methods using tin or stannous chloride in hydrochloric acid or by using Raney nickel with ethanol or hydrazine produces 5-aminoacenaphthene.